Rock'n Roll Trouble Shooting
Detlef-M. Smilgies, CHESS
Rock'n Roll refers to the semiautomatic line-up macros for lining-up
samples for grazing incidence scattering and for calibrating the
incident angle.
Rock'n Roll works in over 95% of all line-ups, but occasionally there
can be a problem, either due to a non-ideal sample or an operator error.
Here is a trouble shooting list
- Check whether the shutter was open during the line-up scan; if not, redo line up with shutter open
- you can redo "rock" as many times as needed, but do not repeat "roll"
- if "roll does not work (only noise in the scans, no reflected beam), your sample may have poor x-ray reflectivity
- for poor reflectivity samples run rock a couple of times, and then set "samth" and "samz" to ZERO
- Check in the hutch whether something is blocking the beam
- Type "wsam" and compare user values and dial values for motors samz and samth.
- I carefully align the sample stage relative to the beam; these motor positions are saved as "dial" values
- if
values differ by more than 10%, use the "set" command to set the motors
to the dial values: set samz <dial value>;set samth <dial
value>
- use the "mv" command to move motors to zero: mv samz 0; mv samth 0
- Make sure that you use a proper sample name containing only (A-Z, a-z, 0-9, -, _); otherwise an error results
- redo "new" with a proper sample name
- Make sure that you supply the correct sample thickness when using the "new" command
- Check that the shutter is open.
- Run the "rock" and "roll" macros again.
If this does not help
- Remove the sample and carefully line up the sample holder with "rock"; set "samz" and "samth" to ZERO
- Does the sample look flat? rough samples are always hard to align, best by hand